Bruker APEXII CCD diffractometer | 4054 independent reflections |
Radiation source: fine focus sealed tube | 3545 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.017 |
Detector resolution: 0.3333 pixels mm-1 | θmax = 27.4°, θmin = 2.4° |
φ and ω scans | h = −15→11 |
Absorption correction: multi-scan (SADABS; Bruker, 2015) | k = −15→15 |
Tmin = 0.776, Tmax = 0.867 | l = −17→17 |
9718 measured reflections |