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. 2019 Jan 11;75(Pt 2):202–207. doi: 10.1107/S2056989019000458
Bruker APEXII CCD diffractometer 4054 independent reflections
Radiation source: fine focus sealed tube 3545 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.017
Detector resolution: 0.3333 pixels mm-1 θmax = 27.4°, θmin = 2.4°
φ and ω scans h = −15→11
Absorption correction: multi-scan (SADABS; Bruker, 2015) k = −15→15
Tmin = 0.776, Tmax = 0.867 l = −17→17
9718 measured reflections