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High-field EPR spectra of 15 mM TEKPol in CHCl3/TBE/MeOH-D4 (65/35/5 v%) (black) and 10 mM AMUPol in D8-glycerol/D2O/H2O (60/30/10 v%) + 2M 13C-urea (red), both recorded at 100 K with a microwave frequency of 285 GHz. Best fits obtained from the DFT-calculated parameters are shown with black and red dashed lines for TEKPol and AMUPol, respectively. The grey overlays represent the errors reported in Table 1.
