Table 1. Data-collection and refinement statistics.
| Crystal | ORP1 –Rab7 |
|---|---|
| Construct | Rab7 2–195, ORP1 5–152 |
| Data collection | 2016 0314 na12 |
| Beamline | PLS-7A |
| Wavelength (Å) | 0.97950 |
| Space group | P212121 |
| Unit-cell parameters (Å,°) | a = 55.1, b = 117.2, c = 130.5 |
| Resolution range (Å) | 50–2.1 (2.14–2.10) |
| No. of reflections | 282965 |
| No. of unique reflections | 50042 (2496) |
| Multiplicity | 5.7 (5.7) |
| Mean I/σ(I) | 39.3 (7.3) |
| Completeness (%) | 99.1 (99.9) |
| Rmerge (%) | 6.9 (32.4) |
| Wilson B factor (Å) | 29.7 |
| Refinement | |
| Rwork (%) | 19.5 (23.1) |
| Rfree (%) | 23.9 (27.2) |
| R.m.s.d., bond lengths (Å) | 0.008 |
| R.m.s.d., bond angles (°) | 0.926 |
| B factor (Å2) | |
| Overall | 41.3 |
| Molecule A, B (Rab7) | 28.1, 57.3 |
| Molecule C, D (ORP1) | 45.1, 37.1 |
| Ligands (GTP) | 18.6, 43.1 |
| Water | 41.3 |
| No. of non-H atoms | |
| Protein | 4825 |
| Ligand | 66 |
| Solvent | 334 |
| Ramachandran statistics | |
| Favored (%) | 97.5 |
| Disallowed (%) | 0.0 |
| PDB entry | 6IYB |