Table 1.
reflection peak | 020 (nm−1) | 110 (nm−1) | 001 (nm−1) | 012 (nm−1) | 013 (nm−1) | 004 (nm−1) |
---|---|---|---|---|---|---|
shafta | 5.90 ± 0.02 | 13.57 ± 0.01 | 6.23 ± 0.01 | 12.35 ± 0.01 | 18.63 ± 0.01 | 24.52 ± 0.01 |
tip regionb | 6.39 ± 0.23 | 13.78 ± 0.15 | — | 12.32 ± 0.07 | 18.59 ± 0.04 | 24.52 ± 0.08 |
lobster tendonc [43] | 6.62 | 13.54 | 6.14 | 12.27 | 18.59 | 24.54 |
crab tendonc [52] | 6.65 | 13.68 | 12.57 | 18.51 | 24.35 |
aFresh sample (data from beamtime at the ESRF); values from average diffraction pattern based on 1853 single diffraction patterns ± error of the fit (N = 1).
bPreviously frozen sample (data from beamtime at PETRA III); number of diffraction patterns n used for calculation of the mean values ± standard deviations (s.d.): 020: n = 17, 110: n = 38, 012: n = 41, 013: n = 41, 004: n = 22 (N = 1).
cDeproteinized.