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. 2019 Feb 6;9:1477. doi: 10.1038/s41598-018-38047-8

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© The Author(s) 2019

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Relative quantitative composition of products formed by CYP6DE1 in in vitro enzyme assays with different monoterpenes, and GC-MS traces of products extracted from female MPB exposed to different monoterpenes. (a) The percentage profile was calculated from total nanograms based upon response factors of authentic standards. (b,c) The percentage profile was calculated by peak area of the extracted ion chromatogram. Retention indices and mass spectra are shown in Supporting Table S2 and Supporting Figs S3–S7. CYP6DE1 assays were performed with N = 6 replicates; MPB treatment assay were performed with N = 4 replicates.