Table 1.
Crystallographic data and refinement statistics. Values in parentheses are for the highest resolution shell.
| Data statistics | |
| Source | SOLElL-PX1 |
| Wavelength (Ȧ) | 1.2824 |
| Space Group | P65 |
| Unit Cell (Ȧ) | a = b = 89.57 c = 321.61 |
| Resolution (Ȧ) | 50–2.30 (2.43–2.30) |
| Number of Observations | 1300,612 (204,730) |
| Number of Unique Reflections | 128,512 (20,379) |
| Completeness (%) | 99.6 (97.9) |
| Redundancy | 10.1 (10.0) |
| Rmeas (%) | 14.1 (179.2) |
| I/σ | 13.9 (1.00) |
| CC ½ | 99.8 (41.9) |
| SigAno | 1.03 (at 3.08 Ȧ) |
| ccAno (%) | 19 (at 3.08 Ȧ) |
| Refinement Statistics | |
| Rwork | 0.20 |
| Rfree | 0.23 |
| Bond RMSD Length(Ȧ)/Angle (°) | 0.01/1.13 |
| Mean B value (overall, Ȧ2) | 70.22 |
| Protein atoms | 7804 |
| Heterogen atoms Zn/Mn/Cl | 12/12/11 |
| Number of Water Molecules | 662 |
| Ramachandran plot | |
| Favored (%) | 97 |
| Outliers (%) | 0 |