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. 2019 Jan 22;24(3):385. doi: 10.3390/molecules24030385

Table 3.

1H- (600 MHz) and 13C- (150 MHz) NMR and HMBC (500 MHz) data of 2 in CDCl3.

Position 1H 13C HMBC
2 J 3 J
1 4.63, d, J = 7.5 Hz, 1H 78.8 - C3, C10, C12
2 - 142.2 - -
3 5.20, d, J = 7.5 Hz, 1H 124.8 - C1, C12
4 2.20, m, 1H; 2.24, m, 1H 24.4 C3 C6
5 2.35, m, 2H 39.5 - C3, C13
6 - 133.2 - -
7 4.82, dd, J = 10.2, 4.4 Hz, 1H 125 - C5, C9
8 1.87, m, 1H; 2.32, m, 1H 42.4 C7 C6, C10
9 - 37.3 - -
10 5.23, d, J = 16.2 Hz, 1H 139.5 - C1, C14, C15
11 5.56, dd, J = 16.2, 7.5 Hz, 1H 131.2 C1 C9, C13
12 1.65, s, 3H 12.8 C2 C1, C3
13 1.43, s, 3H 15.3 C6 C5, C7
14 1.04, s, 3H 24.9 C9 C8, C10, C15
15 1.06, s, 3H 29.9 C9 C8, C10, C14