Table 3.
Position | 1H | 13C | HMBC | |
---|---|---|---|---|
2 J | 3 J | |||
1 | 4.63, d, J = 7.5 Hz, 1H | 78.8 | - | C3, C10, C12 |
2 | - | 142.2 | - | - |
3 | 5.20, d, J = 7.5 Hz, 1H | 124.8 | - | C1, C12 |
4 | 2.20, m, 1H; 2.24, m, 1H | 24.4 | C3 | C6 |
5 | 2.35, m, 2H | 39.5 | - | C3, C13 |
6 | - | 133.2 | - | - |
7 | 4.82, dd, J = 10.2, 4.4 Hz, 1H | 125 | - | C5, C9 |
8 | 1.87, m, 1H; 2.32, m, 1H | 42.4 | C7 | C6, C10 |
9 | - | 37.3 | - | - |
10 | 5.23, d, J = 16.2 Hz, 1H | 139.5 | - | C1, C14, C15 |
11 | 5.56, dd, J = 16.2, 7.5 Hz, 1H | 131.2 | C1 | C9, C13 |
12 | 1.65, s, 3H | 12.8 | C2 | C1, C3 |
13 | 1.43, s, 3H | 15.3 | C6 | C5, C7 |
14 | 1.04, s, 3H | 24.9 | C9 | C8, C10, C15 |
15 | 1.06, s, 3H | 29.9 | C9 | C8, C10, C14 |