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. Author manuscript; available in PMC: 2019 Nov 21.
Published in final edited form as: J Am Chem Soc. 2018 Nov 8;140(46):15616–15620. doi: 10.1021/jacs.8b10206

Figure 4.

Figure 4.

The major products (7a-h) isolated from C-H insertion experiments using triyne precursors 5a-h. Yields are for isolated, purified (SiO2) material. The nature of the R and R’ groups present in each precursor 5 can be deduced from the structure of each resultant product 7. TMS = trimethylsilyl; tBu = tertiary-butyl.