Figure 4.
The major products (7a-h) isolated from C-H insertion experiments using triyne precursors 5a-h. Yields are for isolated, purified (SiO2) material. The nature of the R and R’ groups present in each precursor 5 can be deduced from the structure of each resultant product 7. TMS = trimethylsilyl; tBu = tertiary-butyl.