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. 2019 Feb 26;9:2766. doi: 10.1038/s41598-019-39435-4

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© The Author(s) 2019

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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(A–E) ⁵⁹Co NMR spectra at 5 K for irradiated samples starting with the lowest flux of 1 × 10¹³ ions/cm² up to 1 × 10¹⁵ ions/cm². The corresponding fluence is written in the graphs. Lines are fits with Gaussian lines to the spectra. Dotted black lines denote the Gaussians representing the off-stoichiometric L2₁ ordered regions of the samples, while the filled light grey line corresponds to the A2-ordered regions of the sample. The thick line in the color of the respective data dots is the sum of all Gaussian lines. (F) Irradiation-dependent weight of the A2 structure type (dark green diamonds), FWHM of the L2₁ phase (orange squares), and the corresponding change in the saturation moment (dark red dots).