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a) Anton Paar Monowave 300 (2009). b) Schematic view of the microwave cavity highlighting dual external (IR) and internal (FO) temperature control and the location of the built‐in camera. The inset shows an image taken by the camera (2 mL liquid volume, magnetic stir bar). Images reproduced with permission from ref. 28b and 76. The operating limits of this instrument were 300 °C and 30 bar pressure.
