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. 2019 Feb 11;116(9):3562–3571. doi: 10.1073/pnas.1821216116

Table 1.

Experimental data used in global fits

Experiment Magnetic field, MHz Residue number* Concentrations, mM
13Cα-CPMG relaxation dispersion 600, 900 4, 5, 8, 9, 10, 11, 12, 14, 16, 17 0.4, 0.75, 1.0
13Cα-δex 800 4, 5, 8, 9, 10, 11, 12, 14, 16, 17 0.05, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1.0, 1.1, 1.2
15N-CPMG relaxation dispersion 600, 900 4, 5, 8, 9, 12, 15, 17 0.4, 0.75, 1
15N-R relaxation dispersion 600, 800 4, 5, 8, 9, 12, 15, 17 1.0
15N-δex 800 4, 5, 8, 9, 12, 15, 17 0.05, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1.0, 1.1, 1.2
N15-R21kHz 800 4, 5, 8, 9, 12, 15, 17 0.05, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1.0, 1.1, 1.2
*

Residues not included in the global fit are those where there is either chemical shift overlap precluding accurate measurement of relaxation dispersion data or where the dispersions are small.