Table 1.
Experimental data used in global fits
Experiment | Magnetic field, MHz | Residue number* | Concentrations, mM |
13Cα-CPMG relaxation dispersion | 600, 900 | 4, 5, 8, 9, 10, 11, 12, 14, 16, 17 | 0.4, 0.75, 1.0 |
13Cα-δex | 800 | 4, 5, 8, 9, 10, 11, 12, 14, 16, 17 | 0.05, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1.0, 1.1, 1.2 |
15N-CPMG relaxation dispersion | 600, 900 | 4, 5, 8, 9, 12, 15, 17 | 0.4, 0.75, 1 |
15N-R1ρ relaxation dispersion | 600, 800 | 4, 5, 8, 9, 12, 15, 17 | 1.0 |
15N-δex | 800 | 4, 5, 8, 9, 12, 15, 17 | 0.05, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1.0, 1.1, 1.2 |
800 | 4, 5, 8, 9, 12, 15, 17 | 0.05, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1.0, 1.1, 1.2 |
Residues not included in the global fit are those where there is either chemical shift overlap precluding accurate measurement of relaxation dispersion data or where the dispersions are small.