Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [La2(C10H8O4)3(H2O)4]·8H2O |
| M r | 1070.05 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 293 |
| a, b, c (Å) | 9.1197 (2), 11.1231 (2), 11.9434 (2) |
| α, β, γ (°) | 107.049 (1), 107.729 (1), 106.622 (1) |
| V (Å3) | 1005.21 (3) |
| Z | 1 |
| Radiation type | Mo Kα |
| μ (mm−1) | 2.18 |
| Crystal size (mm) | 0.08 × 0.06 × 0.05 |
| Data collection | |
| Diffractometer | Nonius KappaCCD |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 4588, 4588, 3751 |
| R int | 0.045 |
| (sin θ/λ)max (Å−1) | 0.649 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.030, 0.068, 1.03 |
| No. of reflections | 4588 |
| No. of parameters | 283 |
| No. of restraints | 18 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 1.76, −0.65 |