Table 4.
Mixing procedure.
| Cumulative Mixing Time (min) | Step of Mixing |
|---|---|
| 0 | NR |
| 2 | ½ Silica + ½ TESPT + ½ amine |
| 7 | ½ Silica + ½ TESPT + ½ amine + TDAE oil |
| 12 | ZnO + Stearic acid + TMQ |
| 15 | Discharge |
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