Table 7.

Limits of Detection (LOD) and Limits of Quantitation (LOQ) for mycotoxins analyzed by LC-MS/MS in environmental samples.

Mycotoxins	LOD (µg/Kg)	LOQ (µg/Kg)	Calibration Range	Recovery (%) ± RSD (n = 3)
Aflatoxin M1	0.06	0.20	0.1–8.1	79 ± 6
Aflatoxin B1	0.06	0.20	0.3–32.1	80 ± 2
Aflatoxin B2	0.06	0.20	0.1–8.0	101 ± 12
Aflatoxin G1	0.10	0.10	0.3–32.4	81 ± 2
Aflatoxin G2	0.12	0.40	0.1–8.0	74 ± 1
Deoxynivalenol	2.70	9.00	3.2–1060	90 ± 2
Deoxynivalenol-3-glucoside	5.41	18.00	5.5–548	85 ± 7
15-Acetyldeoxynivalenol	0.81	2.70	3.3–1100	88 ± 6
3-Acetyldeoxynivalenol	0.81	2.70	3.2–1070	90 ± 1
Deepoxydeoxynivalenol	0.36	1.20	1.7–558	92 ± 5
Nivalenol	4.50	15.00	10.7–1070	83 ± 4
Neosolaniol	0.09	0.30	2.2–740	92 ± 2
Zearalanone	0.45	1.50	3.2–107	85 ± 5
Zearalenone	0.18	0.60	0.5–151	87 ± 3
α-Zearalanol	1.98	6.60	2.0–47.4	83 ± 7
β-Zearalanol	0.93	3.10	1.0–47.2	85 ± 7
β-Zearalenol	1.44	4.80	2.0–47.2	81 ± 1
α-Zearalenol	1.02	3.40	1.0–48.6	89 ± 1
Ochratoxin A	0.06	0.20	2.0–199	103 ± 1
Ochratoxin B	0.09	0.30	1.6–164	99 ± 1
Fumonisin B1	0.51	1.70	8.1–811	64 ± 9
Fumonisin B2	0.36	1.20	8.1–809	70 ± 9
Fumonisin B3	0.45	1.50	2.4–235	66 ± 11
T2 toxin	0.12	0.40	3.2–319	104 ± 4
HT2 toxin	0.27	0.90	3.2–322	98 ± 1
T2 Tetraol	5.41	18.00	7.4–741	87 ± 5
T2 Triol	0.33	1.10	2.2–222	103 ± 6
Monoacetoxyscirpenol	0.12	0.40	1.9–634	93 ± 5
Diacetoxyscirpenol	0.30	1	3.2–322	97 ± 2
Roquefortine C	0.21	0.70	3.5–352	87 ± 4
Griseofulvin	0.09	0.30	2.4–239	94 ± 3
Patulin	1.05	3.50	4.1–405	93 ± 7
Fusarenon-X	4.80	16.00	6.4–319	81 ± 8
Mycophenolic acid	0.21	0.70	2.4–815	101 ± 2
Mevinolin	0.09	0.30	2.4–239	98 ± 1
Sterigmatocystin	0.20	0.60	1.0–101	100 ± 3