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. 2019 Feb 20;17(2):125. doi: 10.3390/md17020125

Table 2.

13C NMR spectroscopic data for 1 to 6 at 100 MHz (δ in ppm).

No. 1 a 2 a 3 a 4 a 5 b 6 a
1 171.0, C 172.1, C 13.7, CH3 15.3, CH3 171.7, C 170.6, C
2 119.1, CH 119.1, CH 123.7, CH 121.8, CH 116.6, CH 118.8, CH
3 155.2, C 155.0, C 134.9, C 135.3, C 160.1, C 155.5, C
4 130.6, CH 130.6, CH 131.6, CH 126.8, CH 51.1, CH2 130.6, CH
5 142.2, C 142.1, C 135.1, C 137.2, C 133.5, C 142.3, C
6 49.9, CH2 49.9, CH2 49.8, CH2 48.8, CH2 128.0, CH 50.0, CH2
7 32.1, CH 32.2, CH 32.1, CH 32.1, CH 38.9, CH 32.1, CH
8 37.8, CH2 37.9, CH2 38.0, CH2 38.0, CH2 175.7, C 37.9, CH2
9 27.9, CH2 28.9, CH2 28.2, CH2 28.1, CH2 17.9, CH3 32.1, CH2
10 27.8, CH2 31.2, CH2 27.0, CH2 27.0, CH2 15.9, CH3 26.9, CH2
11 31.0, CH2 24.8, CH2 35.0, CH2 35.0, CH2 18.4, CH3 36.1, CH2
12 32.4, CH2 42.6, CH2 74.1, CH 74.1, CH 71.0, CH
13 38.1, CH 86.5, C 47.5, CH 47.5, CH 56.2, CH
14 80.2, CH 36.5, CH2 179.7, C 179.5, C 175.1, C
15 58.2, CH 44.6, CH 17.0, CH3 24.2, CH3 19.9, CH3
16 172.1, C 179.5, C 17.9, CH3 17.8, CH3 18.5, CH3
17 19.8, CH3 19.8, CH3 20.0, CH3 19.9, CH3 19.8, CH3
18 18.5, CH3 18.5, CH3 13.9, CH3 13.8, CH3 61.6, CH2
19 19.9, CH3 19.9, CH3
20 15.3, CH3 25.5, CH3
21 58.3, CH2 61.0, CH2
OMe 51.9, CH3 52.0, CH3

a Measured in CD3OD; b Measured in CDCl3.