Table 2.
No. | 1 a | 2 a | 3 a | 4 a | 5 b | 6 a |
---|---|---|---|---|---|---|
1 | 171.0, C | 172.1, C | 13.7, CH3 | 15.3, CH3 | 171.7, C | 170.6, C |
2 | 119.1, CH | 119.1, CH | 123.7, CH | 121.8, CH | 116.6, CH | 118.8, CH |
3 | 155.2, C | 155.0, C | 134.9, C | 135.3, C | 160.1, C | 155.5, C |
4 | 130.6, CH | 130.6, CH | 131.6, CH | 126.8, CH | 51.1, CH2 | 130.6, CH |
5 | 142.2, C | 142.1, C | 135.1, C | 137.2, C | 133.5, C | 142.3, C |
6 | 49.9, CH2 | 49.9, CH2 | 49.8, CH2 | 48.8, CH2 | 128.0, CH | 50.0, CH2 |
7 | 32.1, CH | 32.2, CH | 32.1, CH | 32.1, CH | 38.9, CH | 32.1, CH |
8 | 37.8, CH2 | 37.9, CH2 | 38.0, CH2 | 38.0, CH2 | 175.7, C | 37.9, CH2 |
9 | 27.9, CH2 | 28.9, CH2 | 28.2, CH2 | 28.1, CH2 | 17.9, CH3 | 32.1, CH2 |
10 | 27.8, CH2 | 31.2, CH2 | 27.0, CH2 | 27.0, CH2 | 15.9, CH3 | 26.9, CH2 |
11 | 31.0, CH2 | 24.8, CH2 | 35.0, CH2 | 35.0, CH2 | 18.4, CH3 | 36.1, CH2 |
12 | 32.4, CH2 | 42.6, CH2 | 74.1, CH | 74.1, CH | 71.0, CH | |
13 | 38.1, CH | 86.5, C | 47.5, CH | 47.5, CH | 56.2, CH | |
14 | 80.2, CH | 36.5, CH2 | 179.7, C | 179.5, C | 175.1, C | |
15 | 58.2, CH | 44.6, CH | 17.0, CH3 | 24.2, CH3 | 19.9, CH3 | |
16 | 172.1, C | 179.5, C | 17.9, CH3 | 17.8, CH3 | 18.5, CH3 | |
17 | 19.8, CH3 | 19.8, CH3 | 20.0, CH3 | 19.9, CH3 | 19.8, CH3 | |
18 | 18.5, CH3 | 18.5, CH3 | 13.9, CH3 | 13.8, CH3 | 61.6, CH2 | |
19 | 19.9, CH3 | 19.9, CH3 | ||||
20 | 15.3, CH3 | 25.5, CH3 | ||||
21 | 58.3, CH2 | 61.0, CH2 | ||||
OMe | 51.9, CH3 | 52.0, CH3 |
a Measured in CD3OD; b Measured in CDCl3.