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. 2018 Mar 6;26(3):554–562. doi: 10.1016/j.sjbs.2018.03.002

Table 1.

1H NMR spectral data of the 16-hydroxy betulinic acid (300 MHz, δ, CDCl3) with reference to Stefan and Dieter (2009).

Position δH Position δH
1 0.84 (s) 17
2 1.24 (m) 18 1.80 (m)
3 3.48 (t) 19 3.52 (m)
4 20
5 0.83 (m) 21
6 1.26 (m) 22 1.80 (m)
7 23 1.21 (s)
8 24 1.01 (s)
9 1.28 (t) 25 0.83 (s)
10 26 1.13 (s)
11 1.18 (m) 27 1.12 (s)
12 1.15 (m) 28
13 2.46 (m) 29 4.39(br.s)/4.41(br.s)
14 30 1.77 (s)
15 1.80 (m) COOH 7.53 (s)
16 5.18 (d) OH 7.74 (s)