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. Author manuscript; available in PMC: 2020 Jan 10.
Published in final edited form as: Chem. 2018 Nov 21;5(1):215–226. doi: 10.1016/j.chempr.2018.10.017

Figure 2. Optimization of visible light-mediated formal [3+2] cycloaddition toward 1-aminoNBs and DPV measurements.

Figure 2.

[a]Recov. SM = recovered starting material, approximate values indicate that recovered material was not entirely pure and are provided only for general comparison, [b]Reaction run in absence of light, [c]Reaction run in absence of light at 80 °C, [d]Detailed descriptions of flow and batch setups are provided in the Supplemental Information, [e]Reaction run on 1 g-scale, [f]Values obtained through DPV vs. Ag/AgCl, peak potentials were then converted to vs. SCE (VSCE = VAg/AgCl + (0.241 V −0.197 V)), see Supplemental Information for further details and additional DPV measurements, [g]Measured NMM oxidation potential closely compares to previously reported value.63