Table 2.
1H and 13C NMR spectral data of chlamyphilone (in CDCl3).
Position | δC Mult. | δH (J in Hz) | HMBC * |
---|---|---|---|
1 | 115.3 qC | ||
2 | 151.7 CH | 7.91 d (1.37) | 1, 10, 11 |
4 | 155.1 qC | ||
5 | 114.4 qC | ||
6 | 145.2 qC | ||
7 | 102.9 CH | 5.55 d (1.37) | 6, 9 |
8 | 196.3 qC | ||
9 | 83.1 qC | ||
10 | 196.5 qC | ||
11 | 17.5 CH3 | 2.26 d (0.6) | 2 |
12 | 12.7 CH3 | 1.93 d (0.6) | 4, 6 |
13 | 28.6 CH3 | 1.55 s | 9, 10, 8 |
OH | 3.9 | 8 |
* All correlations represent 2 or 3 bond couplings. Abbreviation, s: singlet, d: doublet, t: triplet, dd: doublet of doublets.