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. 2019 Feb 19;24(4):750. doi: 10.3390/molecules24040750

Table 2.

1H and 13C NMR spectral data of chlamyphilone (in CDCl3).

Position δC Mult. δH (J in Hz) HMBC *
1 115.3 qC
2 151.7 CH 7.91 d (1.37) 1, 10, 11
4 155.1 qC
5 114.4 qC
6 145.2 qC
7 102.9 CH 5.55 d (1.37) 6, 9
8 196.3 qC
9 83.1 qC
10 196.5 qC
11 17.5 CH3 2.26 d (0.6) 2
12 12.7 CH3 1.93 d (0.6) 4, 6
13 28.6 CH3 1.55 s 9, 10, 8
OH 3.9 8

* All correlations represent 2 or 3 bond couplings. Abbreviation, s: singlet, d: doublet, t: triplet, dd: doublet of doublets.