Table 1.
Peak | Rt (min) | λmax (nm) | [M + H]+ | Main Fragment ESI- MSn [Intensity (%)] | Tentative Identification |
---|---|---|---|---|---|
P1 | 34.1 | 520 | 919 | 757(49),449(6),287(13) | Cyanidin-3-(p-coumaroyl-6′-caffeoyl)sophoroside isomer 1 A |
P2 | 36.4 | 520 | 919 | 757(49),449(6),287(13) | Cyanidin-3-(p-coumaroyl-6′-caffeoyl)sophoroside isomer 2 A |
P3 | 38.4 | 522 | 1005 | 757(6),535(11),287(11) | Cyanidin-3-(6-p-coumaroyl)sophoroside-5-(6-malonyl)glucoside A |
P4 | 42.8 | 522 | 757 | 595(100),449(11),287(61) | Cyanidin-3-(6-p-coumaroyl)glucoside-5-glucoside A |
P5 | 43.2 | 530 | 1081 | 919(15),449(6),287(6) | Cyanidin-3-(6-p-coumaroyl-6′-caffeoyl)-5-glucoside isomer1 A |
P6 | 43.9 | 532 | 1167 | 919(44),757(5),287(20) | Cyanidin-3-(6-p-coumaroyl-6′-caffeoyl)sophoroside-5-(6-malonyl)glucoside isomer 1 A |
P7 | 44.6 | 530 | 1167 | 919(27),757(5),287(6) | Cyanidin-3-(6 p-coumaroyl-6′-caffeoyl)sophoroside-5-(6-malonyl)glucoside isomer 2 A |
P8 | 45.5 | 530 | 1081 | 919(100),449(11),287(20) | Cyanidin-3-(6-p-coumaroyl-6′-caffeoyl)sophoroside-5-glucoside isomer2 A |
P9 | 45.9 | 530 | 1065 | 903(20),449(5),287(3) | Cyanidin-3-(6,6′-di p-coumaroyl)sophoroside-5-glucoside A |
P10 | 46.4 | 526 | 1151 | 989(10),903(5),287(5) | Cyanidin-3-(6,6′-di p-coumaroyl)sophoroside-5-(6-malonyl)glucoside A |
P11 | 47.0 | 514 | 1049 | 887(33),433(9),271(5) | Pelargonidin-3-(6,6′-di p-coumaroyl)sophoroside-5-glucoside B |
P12 | 48.0 | 526 | 1167 | 1005(63),919(23),449(8),287(13) | Cyanidin-3-(6- p-coumaroyl-X-malonyl-6′-caffeoyl)sophoroside-5-glucoside A |
P13 | 48.7 | 530 | 1151 | 989(28),449(17),287(5) | Cyanidin-3-(6- p-coumaroyl-X-malonyl-6′-p-coumaroyl)sophoroside-5-glucoside A |
Calibration curves used: A- cyanidin-3-O-glucoside (y = 97,787x − 743,469; R2 = 0.999); B- pelargonidin-3-O-glucoside (y = 43,781x − 275,315; R2 = 0.999).