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. 2017 Aug 2;9(8):330. doi: 10.3390/polym9080330

Table 2.

Peak positions (q) of the small-angle X-ray scattering (SAXS) curves, their respective correlation distances (d), and assignments for phase classification (d1/d2, d1/d3). DXM stands for dexamethasone loaded formulations. The sample compositions are described in Table 1.

Samples q1−1) q2−1) q3−1) d (Å) d1/d2 d1/d3 Classification
OA1 0.80 1.38 1.43 7.85 1.73 1.79 *
DXM-OA1 0.80 1.38 1.43 7.85 1.73 1.79 *
OA2 0.84 1.65 2.47 7.48 1.96 2.94 Lamellar
DXM-OA2 0.83 1.66 2.48 7.57 2.00 3.00 Lamellar
OAP1 0.76 1.52 2.29 8.26 2.00 3.00 Lamellar
DXM-OAP1 0.77 1.53 2.29 8.15 2.00 2.97 Lamellar
OAP2 0.80 1.65 2.49 7.85 2.00 3.10 Lamellar
DXM-OAP2 0.78 1.63 2.41 8.00 2.00 3.00 Lamellar
P1 0.90 0.99 1.55 6.98 1.10 1.72 Hexagonal
DXM-P1 0.89 0.99 1.54 7.05 1.10 1.73 Hexagonal
P2 0.99 1.04 1.72 6.34 1.00 1.73 Hexagonal
DXM-P2 0.99 1.04 1.72 6.34 1.00 1.73 Hexagonal
IM1 0.72 1.25 1.90 8.72 1.73 2.63 Hexagonal
DXM-IM1 0.72 1.25 1.90 8.72 1.73 2.63 Hexagonal
IM2 0.72 1.28 1.75 8.72 1.78 2.43 Hexagonal
DXM-IM2 0.66 1.28 1.87 9.52 1.94 2.83 **

(*) overlapped peaks, classification not possible. (**) values of correlation peaks not found in literature for mesophase’s classification.