Table 2.
Composition of the Stock- and Feed solutions for continuous addition terpolymerization of BMA/F8H2MA/MAH and DMA/F8H2MA/MAH (T = 65 °C).
| mDMA (g) | mBMA (g) | mF8H2MA (g) | mMAH (g) | mAIBN (g) | mMEK (g) | mHFX (g) | |
|---|---|---|---|---|---|---|---|
| Stock Solution (A) | - | 0.448 | 0.722 | 1.33 | 0.03 | 4.53 | 2.79 |
| Monomer Feed Solution (B) | - | 5.5 | 6.2 | 0.8 | --- | 1.133 | 1.0 |
| Initiator Feed Solution (C) | - | - | - | - | 0.033 | 0.5 | 0.5 |
| Stock Solution (A) | 0.707 | - | 0.063 | 1.16 | 0.105 | 3.2 | 5.51 |
| Monomer Feed Solution (B) | 6.497 | - | 4.698 | 1.1 | - | 1.6 | 2.0 |
| Initiator Feed Solution (C) | - | - | - | - | 0.060 | 0.5 | - |
BMA, n-butyl methacrylate; F8H2MA, 1H,1H,2H,2H-perfluorodecyl methacrylate; MAH, maleic anhydride; DMA, n-dodecyl methacrylate; AIBN, 2,2′-azo-bisisobutyronitrile; MEK, methyl ethyl ketone; HFX, 1,3-bis (trifluoromethyl) benzene. For details on the calculated amounts, please see the example in Supplementary Materials.