Table 11.
SEC set up and parameters.
| Component | Description | Parameter |
|---|---|---|
| Eluent | THF p.a. | HPLC-grade |
| Pump | Agilent 1100 Series | Flowrate: 1.000 mL min−1 |
| Injector | Rheodyne 7725i sample loop | Injection volume: 60 µL |
| Oven | Agilent 1100 Series | Temperature: 35 °C |
| Column | 1× PSS SDV 8 × 50 mm pre-column | Particle size: 5 µm |
| 2× PSS SDV 8 × 300 mm Linear M 5µ | Particle size: 5 µm Molar weight range: 50–10,000,000 g mol−1 |
|
| Detector | Agilent 1100 Series VWD | Wavelength: 280 nm |
| Calibration | PSS ReadyCal-Kit Polystyren | Calibration range: 376–2,570,000 g mol−1 |