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. 2019 Feb 26;24(5):828. doi: 10.3390/molecules24050828

Table 2.

GC-MS linkage analysis of barley β-glucan (BBG) and its acid hydrolyzed derivatives.

Samples Peak Area (%) a Relative Molar Ratio c T-Glcp:1,3-Glcp:1,4-Glcp Relative Molar Ratio c T-Glcp:1,3-Glcp:1,4-Glcp
T-Glcp b 1,3-Glcp 1,4-Glcp
BBG 3.99 ± 1.00 14.25 ± 0.15 81.76 ± 0.85 1:3.57:20.49 0.28:1:5.74
BBG_0.05 3.76 ± 0.94 14.15 ± 0.14 82.09 ± 0.80 1:3.77:21.84 0.27:1:5.80
BBG_0.1 13.22 ± 2.99 13.11 ± 0.45 73.68 ± 2.54 1:0.99:5.58 1.01:1:5.62
BBG_0.2 22.46 ± 4.55 9.94 ± 0.58 67.60 ± 3.97 1:0.44:3.01 2.26:1:6.80
BBG_0.2(2) 32.28 ± 5.73 9.24 ± 0.78 58.48 ± 4.94 1:0.29:1.81 3.49:1:6.33

a: calculated from the peak area in the GC-MS total ion chromatograms. b: Glcp, glucopyranose. c: molar ratio was calculated from the ratio of the (peak area)/(MW) of individual PMAAs.