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. 2019 Jan 29;10(11):3237–3241. doi: 10.1039/c8sc05096a

Scheme 5. Scope of [18F]fluorodecarboxylation applying protocol B: aArCHFCO2H (0.028 mmol), PhIO (0.5 equiv.), MeCN (1 mL), 50 °C, 10 min then addition of [18F]TEAF (20–30 MBq) Mn(tmp)Cl (2 mg), DMF (300 μL), 50 °C, 20 min. bArCHFCO2H (0.014 mmol), PhIO (0.5 equiv.), MeCN (1 mL), 50 °C, 10 min then addition of [18F]Mn(tmp)F (841 MBq) DCE (300 μL), 60 °C, 20 min.

Scheme 5