Table 11.
Results of stability studies.
Studies | Average retention time (minutes) | Average peak area (mAu·s) | Average asymmetry of peak | Average number of theoretical plate | RSD (%) of peak area | Recovery (%) | ||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|
Peak 1 | Peak 2 | Peak 1 | Peak 2 | Peak 1 | Peak 2 | Peak 1 | Peak 2 | Peak 1 | Peak 2 | Peak 1 | Peak 2 | |
Potassium guaiacolsulfonate | ||||||||||||
Standard solution | ||||||||||||
0 h | 5.633 | 6.734 | 1607838 | 588052 | 0.92 | 0.91 | 2030 | 2902 | 0.03 | 0.04 | — | — |
24 h at refrigerator | 5.636 | 6.734 | 1607531 | 587210 | 0.92 | 0.90 | 2032 | 2902 | 0.03 | 0.05 | 100.0 | 99.9 |
24 h at 25°C | 5.629 | 6.731 | 1606491 | 585247 | 0.92 | 0.91 | 2028 | 2899 | 0.02 | 0.02 | 99.9 | 99.5 |
Sample solution | ||||||||||||
0 h | 5.630 | 6.736 | 1605436 | 585067 | 0.93 | 0.90 | 2028 | 2903 | 0.01 | 0.01 | — | — |
24 h at refrigerator | 5.631 | 6.730 | 1604722 | 584850 | 0.93 | 0.91 | 2029 | 2898 | 0.02 | 0.01 | 100.0 | 100.0 |
24 h at 25°C | 5.629 | 7.735 | 1603874 | 583290 | 0.92 | 0.91 | 2027 | 2902 | 0.05 | 0.05 | 99.9 | 99.7 |
| ||||||||||||
Sodium benzoate | ||||||||||||
Standard solution | ||||||||||||
0 h | 12.380 | 1906212 | 0.99 | 27250 | 0.06 | — | ||||||
24 h at refrigerator | 12.372 | 1905065 | 0.98 | 27214 | 0.02 | 99.9 | ||||||
24 h at 25°C | 12.366 | 1903771 | 0.99 | 27186 | 0.01 | 99.9 | ||||||
Sample solution | ||||||||||||
0 h | 12.375 | 1904980 | 0.99 | 27226 | 0.01 | — | ||||||
24 h at refrigerator | 12.381 | 1904544 | 0.99 | 27249 | 0.02 | 100.0 | ||||||
24 h at 25°C | 12.367 | 1903276 | 0.99 | 27192 | 0.01 | 99.9 |