Table 8.
No. of sample solution | Sample weight (g) | Content of potassium guaiacolsulfonate in oral powder (%, comparing to labeled amount) | Content of sodium benzoate in oral powder (%, comparing to labeled amount) |
---|---|---|---|
Day 1, analyst 1 | |||
1 | 0.6152 | 98.1 | 101.8 |
2 | 0.6224 | 100.8 | 100.0 |
3 | 0.6369 | 99.6 | 101.1 |
4 | 0.6102 | 98.7 | 102.7 |
5 | 0.6224 | 100.7 | 99.9 |
6 | 0.6394 | 99.4 | 100.8 |
Average (1–6) | 99.6 | 101.0 | |
RSD (%) (1–6) | 1.1 | 1.1 | |
| |||
Day 2, analyst 2 | |||
7 | 0.6542 | 100.3 | 101.9 |
8 | 0.6395 | 99.2 | 101.5 |
9 | 0.6452 | 101.3 | 101.3 |
10 | 0.6531 | 100.4 | 102.3 |
11 | 0.6407 | 99.0 | 101.3 |
12 | 0.6446 | 101.6 | 99.4 |
Average (1–12) | 99.9 | 101.2 | |
RSD (%) (1–12) | 1.1 | 1.0 |
Note: results obtained in day 1 by analyst 1 (sample no. 1–6) were used for evaluating repeatability, and those obtained in day 1 and day 2 (sample no. 1–12) were used together for evaluating intermediate precision.