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. 2017 Jun 28;9(7):250. doi: 10.3390/polym9070250

Table 1.

Analytical methods for determining particle distribution in composites manufactured by RTM.

Method Abbreviation Main Area of Use Advantages Disadvantages
transmission electron microscopy TEM fully cured parts qualitative analysis sample preparation
scanning electron microscopy SEM fully cured parts qualitative analysis sample preparation
wavelength dispersive spectrometry SEM/WDS fully cured parts qualitative/quantitative analysis sample preparation
electron probe microanalysis SEM/EPMA fully cured parts qualitative/quantitative analysis sample preparation
burn-off - fully cured parts quantitative analysis total calcination
X-ray computed tomography X-ray CT uncured/cured parts non-destructive small specimens
confocal fluorescence microscopy CFM uncured/cured parts large experimental areas lower resolution than SEM, autofluorescence, fluorescent particle needed
confocal laser scanning microscopy CLSM uncured/cured parts more information about fibres than in case of CRI lower resolution than CRI
confocal Raman imaging CRI uncured/cured parts chemical map, small particles detected time consuming, fluorescent noise