Figure 5.

Two integrals of normalized ASAXS and SAXS Kratky plots have been calculated for four different cubic confinements (1, 2, 4, and 6.5 nm) under the condition of a standard small-angle scattering experiment over the two integration intervals 0< q < 10 nm⁻¹ (a) and 0< q < 2 nm⁻¹ (b). The grey parallelogram represents the area of small confinements with low filling degrees compatible with results from the RI-analysis and XANES (see text).