Table 1.
Compound | 1 |
---|---|
Chemical formula | C30H41N6O13Tb |
M/gmol−1 | 852.61 |
T(K) | 100(2) |
λ/Å | 0.71073 |
Crystal system | Triclinic |
Space group | P-1 |
a/Å | 9.7799(5) |
b/Å | 11.5661(7) |
c/Å | 16.7597(10) |
α/deg | 105.886(2) |
β/deg | 100.772(2) |
γ/deg | 100.290(2) |
V/Å3 | 1,737.46(17) |
Z | 2 |
ρcalcd (g·cm−3) | 1.630 |
μ(mm−1) | 2.108 |
R(int) | 0.0741 |
GOF on F2 | 1.026 |
R1 [I > 2σ(I)] | 0.0544 |
wR2 [I > 2σ(I)] | 0.1173 |
R1 = Σ||F0|–|Fc||/Σ|F0|; wR2 = [Σw(F02 – Fc2)2/ΣwF02]1/2.