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Comparison of room temperature UV–Vis–NIR diffuse-reflectance spectrum for: (a) {[ZnII(bpy)3][NaRu(C2O4)3]}n (1), {[ZnII(bpy)3](H2O)[LiRu(C2O4)3]}n (2) and [Zn(bpy)3](ClO4)2; (b) {[CuII(bpy)3][MIRu(C2O4)3]}n and [CuII(bpy)3](ClO4)2 (MI = Na (3), Li (4)); (c) {[RuII(bpy)3][MIRu(C2O4)3]}n and [Ru(bpy)3](ClO4)2 (MI = Na (5), Li (6)); (d) {[OsII(bpy)3][MIRu(C2O4)3]}n and [Os(bpy)3](PF6)2 (MI = Na (7), Li (8)).
