Table 2.
13C NMR data (100 MHz) of compounds 1−3 and muraymycin C1.
| no. | 1a | 2a, b | 3c | C1c | no. | 1a | 2a, b | 3c | C1c |
|---|---|---|---|---|---|---|---|---|---|
| 1 | 141.6, CH | 141.5, CH | 141.9, CH | 142.3, CH | 21 | 53.4, CH | 53.4, CH | 56.1, CH | 56.0, CH |
| 2 | 101.7, CH | 101.7, CH | 101.9, CH | 102.2, CH | 22 | 75.0, CH | 75.0, CH | 74.4, CH | 74.6, CH |
| 3 | 163.1, C | 163.1, C | 165.9, C | 165.9, C | 23 | 27.8, CH | 27.8, CH | 29.1, CH | 29.2, CH |
| 4 | 150.3, C | 150.3, C | 151.2, C | 151.2, C | 24 | 15.7, CH3 | 15.7, CH3 | 14.6, CH3 | 14.7, CH3 |
| 5 | 90.6, CH | 90.6, CH | 91.1, CH | 91.8, CH | 25 | 19.6, CH3 | 19.6, CH3 | 18.7, CH3 | 18.7, CH3 |
| 6 | 72.6, CH | 72.5, CH | 72.8, CH | 72.5, CH | 26 | 169.5, C | 169.5, C | 171.2, C | 171.1, C |
| 7 | 70.0, CH | 69.9, CH | 69.0, CH | 69.1, CH | 27 | 54.8, CH | 54.8, CH | 55.3, CH | 55.4, CH |
| 8 | 82.8, CH | 82.8, CH | 83.4, CH | 83.7, CH | 28 | 50.0, CH | 50.0, CH | 49.1, CH | 49.1, CH |
| 9 | 76.3, CH | 76.3, CH | 76.4, CH | 76.3, CH | 29 | 20.4, CH2 | 20.4, CH2 | 20.3, CH2 | 20.3, CH2 |
| 10 | 62.5, CH | 62.5, CH | 63.6, CH | 62.8, CH | 30 | 35.6, CH2 | 35.6, CH2 | 35.6, CH2 | 35.7, CH2 |
| 11 | 168.8, C | 168.7, C | 169.9, C | 170.3, C | 31 | 153.7, C | 153.7, C | 153.6, C | 153.6, C |
| 12 | 105.2, CH | 105.1, CH | 106.5, CH | 106.7, CH | 32 | 157.5, C | 157.5, C | 158.7, C | 158.7, C |
| 13 | 84.1, CH | 84.1, CH | 83.9, CH | 83.6, CH | 33 | 173.7, C | 173.6, C | 177.3, C | 176.4, C |
| 14 | 71.8, CH | 71.7, CH | 70.1, CH | 70.5, CH | 34 | 57.5, CH | 57.5, CH | 59.4, CH | 58.6, CH |
| 15 | 79.3, CH | 79.3, CH | 82.9, CH | 79.6, CH | 35 | 30.3, CH | 30.3, CH | 30.1, CH | 29.9, CH |
| 16 | 42.1, CH | 42.0, CH | 41.7, CH | 42.2, CH | 36 | 19.1, CH3 | 19.1, CH3 | 18.5, CH3 | 18.3, CH3 |
| 17 | 45.5, CH2 | 45.5, CH2 | 45.4, CH2 | 45.6, CH2 | 37 | 17.4, CH3 | 17.4, CH3 | 16.6, CH3 | 16.6, CH3 |
| 18 | 25.5, CH2 | 25.4, CH2 | 25.2, CH2 | 25.0, CH2 | 14-OCH3 | 57.5, CH3 | 57.4, CH3 | 57.8, CH3 | 57.9, CH3 |
| 19 | 36.1, CH2 | 36.0, CH2 | 35.8, CH2 | 35.8, CH2 | 16-NHCOCH3 | 174.1, C | |||
| 20 | 169.2, C | 169.1, C | 172.5, C | 172.5, C | 16-NHCOCH3 | 21.9, CH3 | |||
| Fatty acid part for 1 | ![]() |
Fatty acid part for 2 | ![]() |
||||||
measured in DMSO-d6;
measured at 150 MHz;
measured in D2O.

