Scheme 3.
Rapid Synthesis of Fluopyram/Analogsa
aReaction conditions: haloarene (3.0 mmol), olefin (1.0 mmol), PTH (5 mol %), CySH (5 mol %), sodium formate (3.0 mmol), 5% (v/v) H2O/ DMSO (10.0 mL), blue light, 16 h; isolated yields are given.
Rapid Synthesis of Fluopyram/Analogsa
aReaction conditions: haloarene (3.0 mmol), olefin (1.0 mmol), PTH (5 mol %), CySH (5 mol %), sodium formate (3.0 mmol), 5% (v/v) H2O/ DMSO (10.0 mL), blue light, 16 h; isolated yields are given.