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. 2019 Mar 19;75(Pt 3):242–261. doi: 10.1107/S2059798319003528
  B1 B2 B3 B4
Data collection        
Exposure time (s) 0.02 0.02 0.02 0.02
Ω width (°) 0.15 0.15 0.15 0.15
Transmission (%) 1.52 2.90 0.80 1.52
Number of images 1200 600 2400 1200
Data processing        
Crystal parameters        
Space group I213 I213 I213 I213
Unit-cell parameters (Å) a = b = c = 77.47 a = b = c = 77.47 a = b = c = 77.50 a = b = c = 77.51
Data statistics        
Resolution range (Å) 38.74–1.60 (1.63–1.60) 38.74–1.60 (1.63–1.60) 38.75–1.60 (1.63–1.60) 54.81–1.60 (1.63–1.60)
No. of unique reflections 10379 (526) 10379 (526) 10389 (521) 10390 (521)
Multiplicity 19.4 (19.5) 9.7 (9.8) 38.8 (39.0) 19.4 (19.5)
R merge 0.142 (1.582) 0.104 (1.186) 0.220 (2.663) 0.142 (1.732)
R meas 0.146 (1.624) 0.110 (1.252) 0.223 (2.698) 0.146 (1.778)
R p.i.m. 0.033 (0.366) 0.035 (0.399) 0.036 (0.430) 0.033 (0.401)
Completeness (%) 100.0 (100.0) 100.0 (100.0) 100.0 (100.0) 100.0 (100.0)
I/σ(I)〉 12.2 (1.7) 11.2 (1.7) 11.4 (1.1) 12.5 (1.6)
CC1/2 0.999 (0.767) 0.999 (0.691) 0.999 (0.701) 0.999 (0.748)
d min for CC1/2 ≃ 0.5 (Å) 1.45 1.47 1.47 1.48