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. 2019 Mar 19;75(Pt 3):242–261. doi: 10.1107/S2059798319003528
  C1 C2 C3 C4
Data collection        
Exposure time (s) 0.02 0.02 0.02 0.02
Ω width (°) 0.15 0.15 0.15 0.15
Transmission (%) 2.90 0.80 1.52 2.90
Number of images 600 2400 1200 600
Data processing        
Crystal parameters        
Space group I213 I213 I213 I213
Unit-cell parameters (Å) a = b = c = 77.45 a = b = c = 77.42 a = b = c = 77.46 a = b = c = 77.47
Data statistics        
Resolution range (Å) 38.72–1.60 (1.63–1.60) 54.74–1.60 (1.63–1.60) 38.73–1.60 (1.63–1.60) 54.78–1.60 (1.63–1.60)
No. of unique reflections 10379 (526) 10359 (517) 10389 (521) 10380 (526)
Multiplicity 9.4 (9.5) 38.3 (38.5) 19.1 (19.0) 9.5 (9.6)
R merge 0.098 (2.400) 0.191 (4.833) 0.129 (3.081) 0.099 (2.511)
R meas 0.103 (2.539) 0.194 (4.897) 0.132 (3.166) 0.105 (2.654)
R p.i.m. 0.033 (0.823) 0.031 (0.787) 0.030 (0.724) 0.034 (0.855)
Completeness (%) 100.0 (100.0) 100.0 (100.0) 100.0 (100.0) 100.0 (100.0)
I/σ(I)〉 12.4 (1.0) 13.6 (0.8) 14.0 (0.9) 12.5 (0.8)
CC1/2 0.999 (0.450) 1.000 (0.474) 1.000 (0.459) 0.999 (0.379)
d min for CC1/2 ≃ 0.5 (Å) 1.58 1.56 1.56 1.59