Table 4.

Positively Charged AAs^a

l-lysine (Lys/K)		l-arginine (Arg/R)		l-histidine (His/H)
α	3.746 (dd, 1H), 5.63, 6.53	α	3.756 (dd, 1H), 5.99, 6.33	Α	3.983 (dd, 1H), 4.91, 7.78
β2	1.907 (dddd, 1H), 5.63, −14.5, 11.36, 5.13	β2	1.901 (dddd, 1H), 5.99, −14.3, 11.4, 4.87	β2	3.244 (ddd, 1H), 4.91, −15.6, 0.915
β3	1.884 (dddd, 1H), 6.53, −14.5, 5.13, 11.4	β3	1.888 (dddd, 1H), 6.33, −14.3, 5.12, 11.6	β3	3.153 (ddd, 1H), 7.78, −15.6, 0.678
γ2	1.499 (ddddd, 1H), 5.13, 11.4, −13.3, 5.45, 10.1	γ2	1.637 (ddddd, 1H), 11.4, 5.12, −13.6, 6.94, 6.99	γ
γ3	1.432 (ddddd, 1H), 11.4, 5.13, −13.3, 9.87, 5.57	γ3	1.711 (ddddd, 1H), 4.87, 11.6, −13.6, 6.97, 6.94	δ1
δ2	1.721 (ddddd, 1H), 9.87, 5.45, −15.6, 6.92, 7.88	δ2	3.234 (ddd, 1H), 6.94, 6.97, −13.6	δ2	7.905 (ddd, 1H), 0.915, 0.678, 1.26
δ3	1.712 (ddddd, 1H), 5.57, 10.1, −15.6, 10.0, 5.45	δ3	3.23 (ddd, 1H), 6.99, 6.94, −13.6	ε1	7.094 (d, 1H), 1.26
ε2	3.014 (ddd, 1H), 6.92, 10.0, −14.8
ε3	3.010 (ddd, 1H), 7.88, 5.45, −14.8

^aNMR parameters determined by HiFSA analysis: δ_H (multiplicity, rel. integrals), J [Hz].