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. Author manuscript; available in PMC: 2020 Apr 5.
Published in final edited form as: Org Lett. 2019 Mar 12;21(7):2317–2321. doi: 10.1021/acs.orglett.9b00602

Scheme 1.

Scope of the Radical Alkylation/Cyclization Processes with Imines.a b

Scheme 1.

aReaction conditions unless otherwise noted: alkylsilicate (1 equiv, 0.3 mmol), imine (2.0 equiv, 0.6 mmol), photocatalyst (2 mol %), DMSO (0.1 M), irradiating with 30 W blue LEDs at 35 °C for 30 min; all yields are isolated yields after purification. bReaction run for 16 h. cReaction conducted on 1 mmol scale with 1 mol % photocatalyst. dReaction conducted on 2 mmol scale with 1 mol % of photocatalyst.