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(A) Addition of H3B·NMeH2 to 2a (10 mol %) to form 3a and 4a, 1,2-F2C6H4 solvent. (B) Synthesis and solid-state structure of the cationic portion of 4. Selected bond lengths (Å) and angles (deg): Rh1–Rh2 2.6421(4); Rh1–B1 2.326(5), Rh1–B2 2.096(6); Rh2–B1 2.107(5), Rh1–B2, 2.328(5); Rh1–C38 2.997(5), B1–N1, 1.59(1), B2–N1 1.56(1); P1–Rh1–Rh2 162.59(3), P2–Rh1–Rh2, 95.31(3).
