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. 2019 Apr 9;10:1650. doi: 10.1038/s41467-019-09248-0

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© The Author(s) 2019

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 2 — Three-dimensional visualization of the chemical and structural change of Li₂Ru_0.5Mn_0.5O₃ (LRMO) before and after extended charge/discharge cycling. Three-dimensional distribution of Ru and Mn of a pristine LRMO and b LRMO after 97 charge/discharge cycles reconstructed by STEM-EDX tomography. c annular dark-field STEM tomographic (ADF-STEM) reconstruction of a LRMO primary particle after 97 cycles. Two cross-sectional images of the three-dimensional reconstruction are presented to demonstrate that a porous structure had developed throughout the particle (also see Supplementary Figs. 2 and 16 and Supplementary Movie 2). (Scale bar: 100 nm)