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. Author manuscript; available in PMC: 2019 Apr 12.
Published in final edited form as: Nucleosides Nucleotides Nucleic Acids. 2015;34(2):114–129. doi: 10.1080/15257770.2014.965256

Table 1.

Phosphoramidites 7a-7j prepared by the phosphitylation of 2a-2d and 6a-6f.

Product Precursor X Y Z B Yield (%)
7a 2a H H H Gi-Bu 95
7b 2b Me H H Gi-Bu 86
7c 2c H H H GPhOAc 77
7d 2d Me H H GPhOAc 63
7e 6a H OMe OMe APhOAc 88
7f 6b Me H H APhOAc 92
7g 6c H H H CPhOAc 92
7h 6d Me H H CPhOAc 91
7i 6e H H H U 86
7j 6f H H H ABz 82