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. Author manuscript; available in PMC: 2019 Jul 27.
Published in final edited form as: J Nat Prod. 2018 Jul 16;81(7):1619–1627. doi: 10.1021/acs.jnatprod.8b00211

Table 2.

13C NMR Data of Compounds 1−7 (100 MHz, CDCl3)

position 1 2 3 4 5 6 7
1 153.5 156.7 156.5 153.5 153.5 156.3 153.6
2 126.9 124.4 124.5 126.8 126.9 124.5 126.8
3 205.2 205.1 205.0 205.2 205.2 204.9 205.2
4 45.8 45.0 45.7 45.9 45.9 45.0 45.9
5 43.7 40.3 40.3 43.8 44.2 40.5 43.9
6 18.9 20.2 20.4 19.05 19.4 20.3 19.2
7 22.7 23.2 23.2 22.7 23.3 23.1 22.9
8 42.7 40.3 40.3 42.4 43.7 40.3 42.8
9 24.9 33.2 33.1 25.1 24.5 32.9 24.8
 10 30.2 27.1 27.1 30.1 29.9 27.0 29.9
 11 27.7 29.5 29.3 27.89 27.6 29.2 27.6
 12 30.0 32.0 30.0 30.9 31.6 31.0 29.2
 13 47.9 45.6 45.0 45.4 45.5 45.6 45.2
 14 49.6 49.3 48.7 48.9 49.2 48.5 49.2
 15 34.4 32.9 32.7 34.4 34.2 33.2 33.7
 16 25.8 28.1 26.9 26.9 27.4 27.1 27.2
 17 43.1 51.1 48.8 44.1 46.8 49.9 48.2
 18 18.6 14.5 15.4 18.2 17.8 15.9 16.1
 19 27.7 29.7 29.6 27.96 29.2 29.5 28.4
 20 144.3 33.3 45.6 44.6 46.7 40.2 42.5
 21 172.5 19.7 111.9 106.2 110.2 74.3 179.9
 22 133.1 51.7 42.0 38.9 37.9 42.4 46.6
 23 147.9 201.4 110.6 110.9 111.7 111.8 198.9
 24 103.0 124.3 144.0 146.2 146.1 144.4 123.1
 25 199.2 154.9 133.8 132.4 132.0 133.5 156.9
 26 31.1 27.7 10.6 10.4 10.4 10.6 27.8
 27 21.4 20.7 171.2 171.2 171.2 171.4 20.9
 28 19.1 21.4 21.3 21.4 21.4 21.3 21.4
 29 18.4 20.4 20.4 19.13 19.1 20.4 19.1
 30 17.1 17.2 18.4 18.6 17.1 18.4
MeO 56.2 55.0 56.1