Table 1.
Data collection and refinement statistics
| CSB WHD–K48-Ub2 | |
|---|---|
| Data collection | |
| Beamline | SPring-8 BL41XU |
| Space group | P21 |
| Cell constants | |
| a, b, c (Å) | 54.2, 101.7, 66.0 |
| α, β, γ (°) | 90.0, 101.8, 90.0 |
| Resolution | 40–2.6 (2.64–2.6) |
| R sym | 0.210 (0.583) |
| I/σI | 7.4 (1.2) |
| Redundancy | 5.4 (2.6) |
| Completeness (%) | 99.6 (95.3) |
| Refinement | |
| Resolution | 40–2.6 |
| No. reflections | 21,345 |
| R work/Rfree | 0.179/0.236 |
| No. atoms | |
| Protein | 5,282 |
| Ligand | 19 |
| Water | 105 |
| Average B (Å2) | |
| Protein | 44.3 |
| Ligand | 59.6 |
| Water | 35.3 |
| Rmsds | |
| Bond lengths (Å) | 0.002 |
| Bond angles (°) | 0.677 |
| Ramachandran plot (%) | |
| Favored | 98.6 |
| Outliers | 0.0 |
Values in parentheses are for the highest resolution shell.