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. Author manuscript; available in PMC: 2019 Apr 24.
Published in final edited form as: Meteorit Planet Sci. 2015 Apr 24;50(5):976–1004. doi: 10.1111/maps.12445

Table 2.

Iris chromite compositions from TEM and SEM EDS.

Normalized Oxide Weight %
Spectrum SiO2 TiO2 Al2O3 V2O3 Cr2O3 Fe2O3 MgO MnO FeO t (nm)
TEM 24 0.00a 1.80 17.90 43.99 2.85 5.69 27.78 100b
TEM 25 0.00a 1.19 19.03 0.48 45.04 2.18 6.15 0.81 25.13 260
TEM 26 1.48 2.48 14.94 47.10 0 5.90 28.10 150
SEM 10 0.73 1.91 14.12 0.57 45.80 3.93 5.75 0.76 26.43 n/a.c
Cations per 4 oxygens
Spectrum Si Ti Al V Cr Fe3+ Mg Mn Fe2+ Fe3+/ΣFe

TEM 24 0.000 0.045 0.695 1.146 0.071 0.279 0.765 0.08
TEM 25 0.000 0.029 0.734 0.006 1.166 0.054 0.300 0.022 0.688 0.07
TEM 26 0.066 0.083 0.789 1.668 0.000 0.394 1.053 0.00
SEM 10 0.024 0.048 0.558 0.008 1.213 0.099 0.287 0.022 0.741 0.12
a

SiO2 contribution removed. If some glass was present in the spectrum, this could influence other elements.

b

We used a thin film correction based on STXM thickness (t) measurements. Where no STXM measurement was available, we assumed a nominal 100 nm correction.

c

We used the XPP matrix correction on SEM measurements.