Table 2. Data collection and refinement statistics.
| GltTk D-Asp | |
|---|---|
| Data collection | |
| Space group | P3221 |
| Cell dimensions | |
| a, b, c (Å) | 116.55, 116.55, 314.77 |
| α, β, γ (°) | 90.00, 90.00 120.00 |
| Resolution (Å) | 48.06-2.80 (2.87-2.80)* |
| Rmeas | 0.11 (>1) |
| CC1/2 | 99.9 (11.7) |
| I / σI | 8.40 (0.98) |
| Completeness (%) | 99.3 (98.9) |
| Redundancy | 5 (4) |
| Refinement | |
| Resolution (Å) | 2.80 |
| No. reflections | 301,077 |
| Rwork/Rfree (%)s | 23.4/27.2 |
| No. of atom | |
| Protein | 9262 |
| PEG/detergent | 181/33 |
| Ligand/ion | 27/9 |
| Water | - |
| B-factors | |
| Protein | 127 |
| PEG/detergent | 147/174 |
| Ligand/ion | 114/117 |
| Water | - |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.008 |
| Bond angles (°) | 1.162 |
*Values in parentheses are for the highest-resolution shell.