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. 2019 Mar 21;10(16):4458–4468. doi: 10.1039/c9sc00691e

Table 2. The effect of reaction temperature on the reduction of benzyl phenyl ether a .

Inline graphic
Entry Temperature (°C) Con (%) Yield (%)
1 2 3 4
1 100 4.3 4.3 4.3
2 b 100 100 100 87.5 0.3 12.2
3 120 25.5 25.5 23.3 0.2 1.9
4 130 55.3 55.3 50.5 0.5 4.3
5 140 88.5 88.5 75.5 1.1 11.9
6 150 100 100 22.4 1.6 73.1
7 160 100 100 6.8 0.9 92.3

aReaction conditions: benzyl phenyl ether (185 mg, 1 mmol), Ni/Al2O3-600 (20 mg), iso-propanol (10 mL), 3 h, stirring at 1000 rpm.

bThe reaction time was 48 h.