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. Author manuscript; available in PMC: 2019 May 3.
Published in final edited form as: J Am Chem Soc. 2018 Feb 5;140(6):2062–2066. doi: 10.1021/jacs.7b13189

Scheme 1. Optimization of the Synthesis of Stannane 5a.

Scheme 1.

a1H-NMR yield was determined using 1,3,5-trimethoxybenzene as an internal standard. The conversion of starting material is indicated in parentheses. bIsolated yield using 1.0 equiv of diethyl allyl phosphate.