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. Author manuscript; available in PMC: 2019 Nov 1.
Published in final edited form as: Anal Bioanal Chem. 2018 Oct 2;410(29):7773–7781. doi: 10.1007/s00216-018-1394-y

Table 4.

Precision and accuracy assessment of DTG QC samples prepared at mid QC level with multiple ratios of hair mass:extraction solvent volume

Hair Mass Solvent Added Ratio (Hair:Solvent) Target Conc Mean Conc % Bias %CV
5 mg 5 mL 1:1 300 pg/mL 270 pg/mL −10.1 3.6
10 mg 5 mL 2:1 300 pg/mL 332 pg/mL 10.6 5.8
25 mg 5 mL 5:1 300 pg/mL 282 pg/mL −6.0 5.5
50 mg 5 mL 10:1 300 pg/mL 334 pg/mL 11.4 4.7