. 2018 Sep 12;140(38):11931–11934. doi: 10.1021/jacs.8b08385

Table 2. N-Substituted Pyrrole Formation by Dehydrogenative Coupling of Alcohols and Ammonia^a.

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Reaction conditions: Catalyst 1 (0.01 mmol), 2,5-hexanediol (1 mmol), primary alcohol (2 mmol), ammonia (7 bar) 150 °C, 24 h, toluene (0.5 mL), NMR yield with mesitylene as internal standard.

Primary alcohol (4 mmol).

1,4-Butanediol (1 mmol).

1-Phenyl-1,4-pentanediol (1 mmol).

1,4-Diphenyl-1,4-butanediol (1 mmol).

Table 2. N-Substituted Pyrrole Formation by Dehydrogenative Coupling of Alcohols and Ammoniaa.

Table 2. N-Substituted Pyrrole Formation by Dehydrogenative Coupling of Alcohols and Ammonia^a.