Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C19H16N4O |
| M r | 316.36 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 150 |
| a, b, c (Å) | 6.5227 (3), 7.8979 (4), 30.7774 (15) |
| β (°) | 95.389 (2) |
| V (Å3) | 1578.51 (13) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 0.69 |
| Crystal size (mm) | 0.30 × 0.24 × 0.04 |
| Data collection | |
| Diffractometer | Bruker D8 VENTURE PHOTON 100 CMOS |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.85, 0.98 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 11542, 3069, 2613 |
| R int | 0.035 |
| (sin θ/λ)max (Å−1) | 0.617 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.039, 0.091, 1.06 |
| No. of reflections | 3069 |
| No. of parameters | 282 |
| H-atom treatment | All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) | 0.19, −0.18 |