Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C23H15NO3 |
| M r | 353.36 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 10.8204 (10), 3.9364 (3), 40.420 (3) |
| β (°) | 97.651 (3) |
| V (Å3) | 1706.3 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.26 × 0.17 × 0.08 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2009 ▸) |
| T min, T max | 0.771, 0.970 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 45734, 3608, 2570 |
| R int | 0.113 |
| (sin θ/λ)max (Å−1) | 0.617 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.074, 0.178, 1.09 |
| No. of reflections | 3608 |
| No. of parameters | 245 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.20, −0.21 |