Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C20H19N3O3 |
| M r | 349.38 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 18.451 (5), 8.169 (5), 11.591 (5) |
| β (°) | 100.059 (5) |
| V (Å3) | 1720.2 (14) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.30 × 0.25 × 0.20 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD area detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2003 ▸) |
| T min, T max | 0.281, 0.397 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 12516, 3381, 2169 |
| R int | 0.056 |
| (sin θ/λ)max (Å−1) | 0.617 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.045, 0.100, 1.02 |
| No. of reflections | 3381 |
| No. of parameters | 238 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.23, −0.19 |