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. 2019 Apr 9;75(Pt 5):600–603. doi: 10.1107/S2056989019004377

Table 2. Experimental details.

Crystal data
Chemical formula C20H19N3O3
M r 349.38
Crystal system, space group Monoclinic, P21/c
Temperature (K) 296
a, b, c (Å) 18.451 (5), 8.169 (5), 11.591 (5)
β (°) 100.059 (5)
V3) 1720.2 (14)
Z 4
Radiation type Mo Kα
μ (mm−1) 0.09
Crystal size (mm) 0.30 × 0.25 × 0.20
 
Data collection
Diffractometer Bruker APEXII CCD area detector
Absorption correction Multi-scan (SADABS; Bruker, 2003)
T min, T max 0.281, 0.397
No. of measured, independent and observed [I > 2σ(I)] reflections 12516, 3381, 2169
R int 0.056
(sin θ/λ)max−1) 0.617
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.045, 0.100, 1.02
No. of reflections 3381
No. of parameters 238
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.23, −0.19

Computer programs: APEX2 and SAINT (Bruker, 2003), SHELXS2018 (Sheldrick, 2008), PLATON (Spek, 2009), SHELXL2018 (Sheldrick, 2015), Mercury (Macrae et al., 2008), PLATON (Spek, 2009) and publCIF (Westrip, 2010).